Course detail
Laboratory Classes in Analytical Chemistry II
FCH-BCA_ANC2_PAcad. year: 2017/2018
Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, ionex chromatography, electrogravimetry.
Supervisor
Learning outcomes of the course unit
After students finished this course, their competence inceased as follows:
1. They were practical introduced with selected analytical methods.
2. Students be able to practical aplly selected technique of determinations.
3. They practise precise work in analytical laboratory, preparation of standard solutions, good laboratory practise with samples.
4. Students will be able to use of necessary calculations and they will be used evaluation of analytical data from using analysis.
Prerequisites
Laboratory course of analytical chemistry I. Practical knowledge of basic laboratory skills: weighing, pipetting, preparation of measuring solutions, titration, filtration.
Co-requisites
Not applicable.
Recommended optional programme components
Not applicable.
Recommended or required reading
Komendová R., Praktikum z analytické chemie II, BCA_ANC2_P, https://www.vutbr.cz/elearning/ (CS)
Šimek Z., Komendová R., Mašek I., Voznica P. : Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)
Sommer L. : Základy analytické chemie I. VUTIUM, Brno 1998. (CS)
Vláčil F. a kol. : Příklady z chemické a instumentální analýzy. INFORMATORIUM, Praha 1991. (CS)
Sommer L. a kol. : Základy analytické chemie II. VUTIUM, Brno 2000. (CS)
Planned learning activities and teaching methods
The course uses teaching methods in form of Laboratory exercise - 4 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.
Assesment methods and criteria linked to learning outcomes
Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test (15-20 questions)
Final classification is based on average classification of individual tasks.
Classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F
Language of instruction
Czech
Work placements
Not applicable.
Course curriculum
1. Introduction to practice, safety of work, methodology of work in analytical laboratory
2. Precipitation titration (Argentometry)
3. Automatic titration (alkalimetry)
4. Titration in a non-aqueous medium
5. Spectrophotometry
6. Multi-component analysis
7. Fluorimetry
8. Emission flame spectrometry
9. Voltammetry and electrogravimetry
10. Extraction spectrophotometry
11. Liquid Chromatography
12. Thin-layer chromatography
Aims
The aim of practical classes of analytical chemistry II is to learn students the base and using of selected analytical instrumental methods, such as potentiometry, automatic titration, spectrophotometry, fluorimetry, emission flame spectrometry, TLC, chromatography and electrogravimetry.
Specification of controlled education, way of implementation and compensation for absences
Input e-learning tests to check students' readiness.
Work in analytical laboratory.
Evaluation of analytical results.
Elaboration of the protocols.
Credit test at the end of the course.
Classification of course in study plans
- Programme BPCP_CHCHT Bachelor's
branch BPCO_SCH , 2. year of study, summer semester, 3 credits, compulsory
- Programme BKCP_CHCHT Bachelor's
branch BKCO_SCH , 2. year of study, summer semester, 3 credits, compulsory
- Programme BPCP_CHCHT Bachelor's
branch BPCO_CHTOZP , 2. year of study, summer semester, 3 credits, compulsory
- Programme BKCP_CHCHT Bachelor's
branch BKCO_CHTOZP , 2. year of study, summer semester, 3 credits, compulsory
- Programme BPCP_CHCHT Bachelor's
branch BPCO_CHMN , 2. year of study, summer semester, 3 credits, compulsory
branch BPCO_CHM , 2. year of study, summer semester, 3 credits, compulsory - Programme BKCP_CHCHT Bachelor's
branch BKCO_CHM , 2. year of study, summer semester, 3 credits, compulsory
- Programme BPCP_CHTP Bachelor's
branch BPCO_BT , 2. year of study, summer semester, 3 credits, compulsory
- Programme BKCP_CHTP Bachelor's
branch BKCO_BT , 2. year of study, summer semester, 3 credits, compulsory
branch BKCO_PCH , 2. year of study, summer semester, 3 credits, compulsory - Programme BPCP_CHTP Bachelor's
branch BPCO_CHP , 2. year of study, summer semester, 3 credits, compulsory
- Programme CKCP_CZV lifelong learning
branch CKCO_CZV , 1. year of study, summer semester, 3 credits, compulsory
Type of course unit
Laboratory exercise
52 hours, compulsory
Teacher / Lecturer