Publication detail

Viscous flow spark plasma sintering of glass microspheres with YAG composition and high tendency to crystallization

MICHÁLKOVÁ, M. KRAXNER, J. PARCHOVIANSKÝ, M. KLEMENT, R. POUCHLÝ, V. MACA, K. GALUSEK, D.

Original Title

Viscous flow spark plasma sintering of glass microspheres with YAG composition and high tendency to crystallization

Type

journal article in Web of Science

Language

English

Original Abstract

Present work is focused on the preparation of bulk glass with stoichiometric yttrium aluminium garnet (YAG) composition, which has high tendency to crystallize. Glass microspheres were prepared by flame synthesis from sol-gel prepared YAG precursor. Sintering conditions in SPS apparatus such as heating rate, pressure and temperature were optimized with the aim to prepare transparent material. Results revealed that glass with high tendency to crystallize is very sensitive to time of densification under load (associated with the maximum applied temperature). The increase of the pressure led to the expansion of the translucent part of the sample. Dense, and slightly translucent amorphous samples (total transmission measured at 550 nm was 4.8 %) were successfully prepared by viscous flow SPS sintering of glass microspheres at temperatures below 910 degrees C without any isothermal dwell.

Keywords

Flame synthesis; Glass; Glass-ceramic; Microspheres; SPS; YAG

Authors

MICHÁLKOVÁ, M.; KRAXNER, J.; PARCHOVIANSKÝ, M.; KLEMENT, R.; POUCHLÝ, V.; MACA, K.; GALUSEK, D.

Released

1. 2. 2021

Publisher

ELSEVIER SCI LTD

Location

OXFORD

ISBN

1873-619X

Periodical

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY

Year of study

41

Number

2

State

United Kingdom of Great Britain and Northern Ireland

Pages from

1537

Pages to

1542

Pages count

6

URL

https://www.sciencedirect.com/science/article/pii/S0955221920308281?via%3Dihub

BibTex

@article{BUT172714,
  author="Monika {Michálková} and Jozef {Kraxner} and Milan {Parchovianský} and Róbert {Klement} and Václav {Pouchlý} and Karel {Maca} and Dušan {Galusek}",
  title="Viscous flow spark plasma sintering of glass microspheres with YAG composition and high tendency to crystallization",
  journal="JOURNAL OF THE EUROPEAN CERAMIC SOCIETY",
  year="2021",
  volume="41",
  number="2",
  pages="1537--1542",
  doi="10.1016/j.jeurceramsoc.2020.10.015",
  issn="1873-619X",
  url="https://www.sciencedirect.com/science/article/pii/S0955221920308281?via%3Dihub"
}