Course detail

Laboratory Classes in Instrumental Analysis

FCH-MC_PIAAcad. year: 2021/2022

Methods of instrumental analysis - realization of given tasks.

Language of instruction

Czech

Number of ECTS credits

3

Mode of study

Not applicable.

Learning outcomes of the course unit

Practice in chosen experimental methods of instrumental and structural analysis

Prerequisites

basic knowledge of analytical and instrumental chemistry

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course uses teaching methods in form of Laboratory exercise - 3 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.

Assesment methods and criteria linked to learning outcomes

Conditions for awarding the course-unit credit is realization of selected tasks and properly kept laboratory notebook. Details are described in e-learning. Requirement for credits are agreement of teachers of the individual tasks - signatures in laboratory notebook.

Course curriculum

Methods of instrumental analysis - realization of given tasks.

0. Introduction

1. Lyophilization and morphologic characterization by SEM
2. Vibrational Spectroscopy I - sampling and measuring techniques
3. Densitometry and viscometry
4. Utilization of microcalorimetry in study of binding and phase equilibriums
5. Fluorescence spectroscopy

6. AFM - atomic force microscopy
7. HRUS - high resolution ultrasound spectroscopy
8. Vibrational Spectroscopy II - qualitative and quantitative analysis
9. Potentiometric and conductometric titrations
10. Methods of anorganic and organic elemental analysis (ICP-OES and EA)

Work placements

Not applicable.

Aims

The aim of the subject is to acquire measuring technique and to acquaint students with practical problems of chosen methods of instrumental analysis.

Specification of controlled education, way of implementation and compensation for absences

Student attends given tasks in agreement with their teachers, which is checked on the basis of the laboratory date-book by garant.

LABORATORY DATE-BOOK
Notes in laboratory date-book are destined for archivation of course and results of laboratory activities. Following details should be included in date-book:
date of record (date of laboratory activity),
name of laboratory activity,
reason of laboratory activity,
description of operating procedure,
all actual data (weights, concentrations, temperatures...),
obtained results (in written or electronic form).
other notes or problems in measurements
number of page

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Čůta, K. a kol.. Instrumentální analýza. SNTL, Praha 1986. (CS)
dle zadání vedoucího vybraného úkolu (CS)

Recommended reading

Not applicable.

eLearning

Classification of course in study plans

  • Programme NPCP_CHCHTE Master's, 1. year of study, winter semester, compulsory
  • Programme NKCP_CHCHTE Master's, 1. year of study, winter semester, compulsory