Course detail
Laboratory Classes in Analytical Chemistry I
FCH-BCA_ANC1_PAcad. year: 2018/2019
Practical training at analytical reaction of selected ions: cations of alkali metals and alkali earth metals, group of cations precipitating by HCl, by sulphane under acidic conditions, by amonium hydrogensufide, group of anions forming precipitates with baryum (II), anions forming precipitates with and with silver (I).
Practical training of basic quantitative analytical methods: gravimetry, acid-base titrations, compleximetric titrations and redox titrations.
Supervisor
Learning outcomes of the course unit
After students finished this course, they increase their competence as follows:
1. They have overview of analytically and technologically significant reactions of common ions.
2. They extension of knowledge on reactivity and some physical properties of groups of elements/ions.
3. Students be able apply the choice of an important analytical reagents and indicators.
4. Students be introduced with techniques of microscope reactions and small-volume reactions.
5. They will be used precise work in analytical laboratory, preparation of standard solutions and samples.
6. Students will be able to use of basic calculations in gravimerty and volumetry.
Prerequisites
Practical knowledge of basic laboratory skills: weighing, pipetting, preparation of solutions, titration, filtration.
Co-requisites
Not applicable.
Recommended optional programme components
Not applicable.
Recommended or required reading
Komendová R.: Praktikum z analytické chemie I, BCA_ANC1_P, https://www.vutbr.cz/elearning/ (CS)
Komendová R., Šenkýř J., Šimek Z.: Analytické reakce anorganických iontů. FCH VUT v Brně, Brno 2003. (CS)
Šimek, Z., Komendová, R., Mašek, I., Voznica, P.: Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)
Sommer L.: Základy analytické chemie I. Skriptum FCH VUT v Brně, VUTIUM Brno 1998 (CS)
Okáč, A.: Analytická chemie kvalitativní. Nakl. ČSAV, Praha 1961 (CS)
Šenkýř, J.: Vybrané postupy k důkazu iontů v kvalitativní analýze. MAsarykova univerzita, Brno 1993. (CS)
Planned learning activities and teaching methods
The course uses teaching methods in form of Laboratory exercise - 4 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.
Assesment methods and criteria linked to learning outcomes
Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test (15-20 questions)
Final classification is based on average classification of individual tasks.
Classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F
Language of instruction
Czech
Work placements
Not applicable.
Course curriculum
1. Introduction, work safety, analytical laboratory techniques
2. Cations of alkali metals and alkaline earth metals
3. Groups of ions precipitating HCl and H2S under acidic conditions.
4. Group of ions precipitated by NH4HS.
5. Group of little soluble Ba2+ salts.
6. Group of anions producing Ag+ salts, soluble in 2 mol/L HNO3
7. Group of anions producing Ag+ salts, little soluble in 2 mol/L HNO3, and NO3-, NO2-, ClO4-
8. Gravimetry - determination of Fe, determination of Ni.
9. Acid-base titrations I.
10. Acid-base titrations II.
11. Compleximetric titrations.
12. Redox titrations.
Aims
The aim of the first part of laboratory classes on analytical chemistry I, focused on quantitative reactions, is to learn students characteristic reactions of anorganic ions with selected group and selective agents, with visual or basic instrumental detection. The aim of the second part of laboratory classes on analytical chemistry I is introduction of students to problems of qualitative analytical chemistry, mastering of basic analytical methods of gravimetry and volumetry.
Specification of controlled education, way of implementation and compensation for absences
Written entrance tests at the beginning of all exercises checking the students readiness for practical work.
The evaluation of analytical results.
Elaboration of the protocols on a given exercises.
Credit test at the course end.
Classification of course in study plans
- Programme BKCP_CHCHT Bachelor's
branch BKCO_SCH , 2. year of study, winter semester, 3 credits, compulsory
- Programme BPCP_CHCHT Bachelor's
branch BPCO_SCH , 2. year of study, winter semester, 3 credits, compulsory
branch BPCO_CHTOZP , 2. year of study, winter semester, 3 credits, compulsory - Programme BKCP_CHCHT Bachelor's
branch BKCO_CHTOZP , 2. year of study, winter semester, 3 credits, compulsory
- Programme BPCP_CHCHT Bachelor's
branch BPCO_CHMN , 2. year of study, winter semester, 3 credits, compulsory
- Programme BKCP_CHCHT Bachelor's
branch BKCO_CHM , 2. year of study, winter semester, 3 credits, compulsory
- Programme BPCP_CHCHT Bachelor's
branch BPCO_CHM , 2. year of study, winter semester, 3 credits, compulsory
- Programme BPCP_CHTP Bachelor's
branch BPCO_BT , 2. year of study, winter semester, 3 credits, compulsory
- Programme BKCP_CHTP Bachelor's
branch BKCO_BT , 2. year of study, winter semester, 3 credits, compulsory
branch BKCO_PCH , 2. year of study, winter semester, 3 credits, compulsory - Programme BPCP_CHTP Bachelor's
branch BPCO_CHP , 2. year of study, winter semester, 3 credits, compulsory
- Programme CKCP_CZV lifelong learning
branch CKCO_CZV , 1. year of study, winter semester, 3 credits, compulsory
Type of course unit
Laboratory exercise
52 hours, compulsory
Teacher / Lecturer
Ing. Hana Barboříková
Ing. Jakub Fojt
Mgr. Petr Chrást
Pavla Kleinová
Mgr. Renata Komendová, Ph.D.
Ing. Eva Matejčíková
Ing. Ludmila Mravcová, Ph.D.
Ing. Václav Pecina
Ing. Veronika Řezáčová, Ph.D.
Ing. Marta Skoumalová
Ing. Petra Suková
Ing. Jiří Sýkora
Ing. Petra Venská
doc. MVDr. Helena Zlámalová Gargošová, Ph.D.
eLearning
eLearning: opened course