Mgr. Renata Komendová, Ph.D.

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

After students finished this course, they increase their competence as follows:

1. They have overview of analytically and technologically significant reactions of common ions.
2. They extension of knowledge on reactivity and some physical properties of groups of elements/ions.
3. Students be able apply the choice of an important analytical reagents and indicators.
4. Students be introduced with techniques of microscope reactions and small-volume reactions.
5. They will be used precise work in analytical laboratory, preparation of standard solutions and samples.
6. Students will be able to use of basic calculations in gravimerty and volumetry.

Practical knowledge of basic laboratory skills: weighing, pipetting, preparation of solutions, titration, filtration.

Not applicable.

Not applicable.

Komendová R.: Praktikum z analytické chemie I, BCA_ANC1_P, https://www.vutbr.cz/elearning/ (CS)
Komendová R., Šenkýř J., Šimek Z.: Analytické reakce anorganických iontů. FCH VUT v Brně, Brno 2003. (CS)
Šimek, Z., Komendová, R., Mašek, I., Voznica, P.: Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)
Sommer L.: Základy analytické chemie I. Skriptum FCH VUT v Brně, VUTIUM Brno 1998 (CS)
Okáč, A.: Analytická chemie kvalitativní. Nakl. ČSAV, Praha 1961 (CS)
Šenkýř, J.: Vybrané postupy k důkazu iontů v kvalitativní analýze. MAsarykova univerzita, Brno 1993. (CS)

The course uses teaching methods in form of Laboratory exercise - 4 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test (15-20 questions)
Final classification is based on average classification of individual tasks.
Classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F

Czech

Not applicable.

1. Introduction, work safety, analytical laboratory techniques
2. Cations of alkali metals and alkaline earth metals
3. Groups of ions precipitating HCl and H2S under acidic conditions.
4. Group of ions precipitated by NH4HS.
5. Group of little soluble Ba2+ salts.
6. Group of anions producing Ag+ salts, soluble in 2 mol/L HNO3
7. Group of anions producing Ag+ salts, little soluble in 2 mol/L HNO3, and NO3-, NO2-, ClO4-
8. Gravimetry - determination of Fe, determination of Ni.
9. Acid-base titrations I.
10. Acid-base titrations II.
11. Compleximetric titrations.
12. Redox titrations.

The aim of the first part of laboratory classes on analytical chemistry I, focused on quantitative reactions, is to learn students characteristic reactions of anorganic ions with selected group and selective agents, with visual or basic instrumental detection. The aim of the second part of laboratory classes on analytical chemistry I is introduction of students to problems of qualitative analytical chemistry, mastering of basic analytical methods of gravimetry and volumetry.

Written entrance tests at the beginning of all exercises checking the students readiness for practical work.
The evaluation of analytical results.
Elaboration of the protocols on a given exercises.
Credit test at the course end.

• Programme BKCP_CHCHT Bachelor's

  branch BKCO_SCH , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BPCP_CHCHT Bachelor's

  branch BPCO_SCH , 2. year of study, winter semester, 3 credits, compulsory
  branch BPCO_CHTOZP , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BKCP_CHCHT Bachelor's

  branch BKCO_CHTOZP , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BPCP_CHCHT Bachelor's

  branch BPCO_CHMN , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BKCP_CHCHT Bachelor's

  branch BKCO_CHM , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BPCP_CHCHT Bachelor's

  branch BPCO_CHM , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BPCP_CHTP Bachelor's

  branch BPCO_BT , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BKCP_CHTP Bachelor's

  branch BKCO_BT , 2. year of study, winter semester, 3 credits, compulsory
  branch BKCO_PCH , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme BPCP_CHTP Bachelor's

  branch BPCO_CHP , 2. year of study, winter semester, 3 credits, compulsory
  

• Programme CKCP_CZV lifelong learning

  branch CKCO_CZV , 1. year of study, winter semester, 3 credits, compulsory
  

52 hours, compulsory

Ing. Hana Cigánková
Ing. Jakub Fojt
Mgr. Petr Chrást
Pavla Kleinová
Mgr. Renata Komendová, Ph.D.
Ing. Eva Matejčíková
Ing. Ludmila Mravcová, Ph.D.
Ing. Václav Pecina
Ing. Veronika Řezáčová, Ph.D.
Ing. Marta Skoumalová
Ing. Petra Suková
Ing. Jiří Sýkora
Ing. Petra Venská
doc. MVDr. Helena Zlámalová Gargošová, Ph.D.