Course detail

Experimental Methods in Materials Engineering

FSI-WEMAcad. year: 2017/2018

Basic methods for the preparation, observation and evaluation of the structure of metallic and non-metallic (ceramics, composites, plastics, concretes, wood) materials, using modern analytical methods (light and electron microscopies, X-ray analysis, spectroscopy, etc.). Assessment of the relations between the structure and the mechanical and physical properties of materials. The students will further be made familiar with the evaluation of the structure of a material on the basis of current standards, and they will apply their knowledge to practical problems.

Language of instruction

Czech

Number of ECTS credits

8

Mode of study

Not applicable.

Guarantor

Ing. Lenka Klakurková, Ph.D.

Department

Institute of Materials Science and Engineering (ÚMVI)

Learning outcomes of the course unit

The knowledge of the principles and application potentials of the basic methods of structure and phase analysis, inclusive of procedures of taking and preparing specimens. Separate evaluation of structure components for all the kinds of materials under study, and assessment of the relations between the production technology, structure, and useful properties of materials.

Prerequisites

The study of the experimental methods used in the structure analysis (morphology and phase composition) of materials requires the basic knowledge of physics and mathematics on the level offered in the course of bachelor studies, and also knowledge of materials science and engineering – on the level of BSc at the least.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course is taught through lectures explaining the basic principles and theory of the discipline. Teaching is suplemented by practical laboratory work.

Assesment methods and criteria linked to learning outcomes

Exam: written and oral parts. Awarding the course-unit credit is conditional on the elaboration of protocols, full attendance and credit test.

Course curriculum

Not applicable.

Work placements

Not applicable.

Aims

The goal of the course is to give students a survey and, to a lesser extent, the theoretical knowledge and principles of all the basic methods for the structure and phase analysis (physical principles of the methods, instrument parameters, application scope of the methods, etc.), inclusive of specimen preparation.

Specification of controlled education, way of implementation and compensation for absences

Attendance at seminars is compulsory. Absence from seminars may be compensated for by the agreement with the teacher.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

SKOČOVSKÝ, Petr a Tomáš PODRÁBSKÝ. Farebná metalografia zliatin železa. Žilina: Žilinská univerzita, 2001. ISBN 80-7100-911-3. (SK)

Recommended reading

Not applicable.

Classification of course in study plans

  • Programme B3A-P Bachelor's

    branch B-MTI , 2. year of study, winter semester, compulsory

Type of course unit

 

Lecture

39 hours, optionally

Teacher / Lecturer

Ing. Lenka Klakurková, Ph.D.

Syllabus

1. Macro, micro, nano its structure and study for research and practice
2. Light microscopy (color contrast, micro-hardness phase, etc.)
3. Introduction to electron microscopy (TEM) sample preparation for EM
4. Electron microscopy REM, EBSD, FIB, etc.
5. Microanalysis of the chemical composition by EDS, WDS, EELS etc.
6. X-ray diffraction phase analysis (description, usage), diffraction analysis
7. Methods spectroscopic chemical analysis
8. Evaluation of defects in molded blanks and castings, evaluation and microcleaness micropurity materials
9. Evaluation of microstructural parameters according to standards, ČSNEN, ASTM
10. Rating layers after the heat, respectively. chemical and thermal processing, evaluation of welded joints etc.
11. Methods of quantitative evaluation phase using image analysis (SM, EM)
12. Materialography of polymers, including of wood
13. Introduction " FailureAnalysis "

Exercise

16 hours, compulsory

Teacher / Lecturer

Ing. Lenka Klakurková, Ph.D.

Syllabus

1. Preparation of samples for light and electron microscopy
2. Practical observation and evaluation structure of materials using the SM ( use of color contrast )
3. Examples use TEM ( substructure , defects, diffraction)
4. End-of-term test, awarding of credits.

labs and studios

36 hours, compulsory

Teacher / Lecturer

Ing. Lenka Klakurková, Ph.D.

Syllabus

1 Application of physical methods (dilatometry, resistivity, magnetometry)
2. Application of local chemical microanalysis in TEM and SEM (EDS and WDS)
3. X-ray phase analysis - demonstrations of applications, calculation parameters grids etc.,
4. The use of spectroscopic chemical analysis in practice - examples of applications
5. Introduction to Quantitative metallography, cast iron structure evaluation
6. Evaluation of defects formed blanks and castings, makročistota and Micro-purity materials - practical applications
7. Evaluation of microstructural parameters - practical applications
8. Determining the size of a grain of steels and nonferrous alloys using different methods and standards
9. Practical application evaluation microstructural parameters using the modules available image analysis (Olympus - StreamMotion)