Publication detail

The Effect of Post-Treatment on the Composition of Formed Negative Electrode Mass in Lead Acid Batteries Studied by XRD

ČECH, O. CHLADIL, L. VANÝSEK, P. ZIMÁKOVÁ, J. KŘIVÍK, P. VACULÍK, S. BAČA, P.

Original Title

The Effect of Post-Treatment on the Composition of Formed Negative Electrode Mass in Lead Acid Batteries Studied by XRD

Type

journal article in Web of Science

Language

English

Original Abstract

Ex-situ investigation of the structure of negative lead-acid electrodes faces the problem of fast electrode degradation when taken out of the electrolyte. Examining the formed negative electrode structure, whether by optical, chemical, or crystallographic means, retains its central purpose only if the electrode structure is preserved unchanged, at least during the measurement itself. The research showed that an appropriate choice of the solvent to wash the electrode after extraction from the cell is a crucial factor; the best results were obtained when using ethanol in combination with drying in a nitrogen atmosphere.

Keywords

Lead-acid, XRD, PbSO4, Tribasic, Lead sulfate, Washing

Authors

ČECH, O.; CHLADIL, L.; VANÝSEK, P.; ZIMÁKOVÁ, J.; KŘIVÍK, P.; VACULÍK, S.; BAČA, P.

Released

18. 9. 2017

Publisher

Elsevier

ISBN

2352-152X

Periodical

Journal of Energy Storage

Year of study

1

Number

1

State

Kingdom of the Netherlands

Pages from

1

Pages to

5

Pages count

5

URL

http://www.sciencedirect.com/science/article/pii/S2352152X17301329?via%3Dihub

BibTex

@article{BUT139993,
  author="Ondřej {Čech} and Ladislav {Chladil} and Petr {Vanýsek} and Jana {Zimáková} and Petr {Křivík} and Sebastian {Vaculík} and Petr {Bača}",
  title="The Effect of Post-Treatment on the Composition of Formed Negative Electrode Mass in Lead Acid Batteries Studied by XRD",
  journal="Journal of Energy Storage",
  year="2017",
  volume="1",
  number="1",
  pages="1--5",
  doi="10.1016/j.est.2017.07.030",
  issn="2352-152X",
  url="http://www.sciencedirect.com/science/article/pii/S2352152X17301329?via%3Dihub"
}